Ultrasound-assisted ionic liquid-based dispersive liquid-liquid microextraction procedure for preconcentration of cobalt and nickel in environmental and biological samples prior to FAAS determination
نویسندگان
چکیده
منابع مشابه
Determination of Cobalt in Food, Environmental and Water Samples with Preconcentration by Dispersive Liquid-Liquid Microextraction
A new method for the determination of cobalt was developed by dispersive liquid-liquid microextraction preconcentration and flame atomic absorption spectrometry. In the proposed approach, 1,5-bis(di-2-pyridyl) methylene thiocarbohydrazide (DPTH) was used as a chelating agent, and chloroform and ethanol were selected as extraction and dispersive solvents. Some factors influencing the extraction ...
متن کاملPreconcentration and determination of palladium water samples by ionic liquid - dispersive liquid liquid microextraction combined with flame atomic absorption spectrometry
A simple, rapid and efficient dispersive liquid–liquid microextraction by use of ionic liquid (IL-DLLME)method, followed by flame atomic absorption spectrometry (FAAS) was developed for the preconcentrationand determination of palladium in water samples. In this method, an appropriate mixture of acetone and octylmethyl imidazolium hexafluorophosphate was injected rapidly into the aqueous sample...
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In this study, we combined Ionic Liquid-based Dispersive Liquid Liquid Micro Extraction (IL-DLLME) with FAAS for determining the palladium in different real samples at the trace level. 1-hexyl-3-methylimidazolium hexafluorophosphate [Hmim][PF6] ionic liquid and 1-(2-pyridylazo) 2-naphthol (PAN), were chosen as the extraction solvent and the chelating agent, respectively. The hydr...
متن کاملSpectrophotometric Determination of Copper and Nickel in Marine Brown Algae after Preconcentration with Surfactant Assisted Dispersive Liquid-Liquid Microextraction
A simple, fast and effective pre-concentration method for the determination of Cu (copper) and Ni (nickel) was developed using a Surfactant Assisted Dispersive Liquid-Liquid Microextraction (SA-DLLME) coupled by UV-Vis spectrophotometry in marine brown algae. The complexing agent was 1- (2- pyridylazo) – 2 - naphthol (PAN).The effects of various experimental parameters in the extraction ste...
متن کاملIonic Liquid-based Ultrasound-assisted In-situ Solvent Formation Microextraction and High-performance Liquid Chromatography for the Trace Determination of Polycyclic Aromatic Hydrocarbons in Environmental Water Samples
A green and efficient ionic liquid-based ultrasound-assisted in-situ solvent formationmicroextraction (IL-UA-ISFME) in combination with high-performance liquid chromatographyultravioletdetection (HPLC-UV) has been successfully developed for the trace determination offive selected polycyclic aromatic hydrocarbons (PAHs) in environmental water samples. In thismethod, a hydrophobic ionic liquid (1...
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ژورنال
عنوان ژورنال: Egyptian Journal of Advanced Applied Sciences
سال: 2022
ISSN: ['1110-1555']
DOI: https://doi.org/10.21608/bfszu.2022.135282.1130